HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Methylguanidino)-4-(3-aminocyclohexyl)thiazole → HCID 178485102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Methylguanidino)-4-(3-aminocyclohexyl)thiazole | HCID 20530385 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178485102 | HCID 178485102 | — |
Reaction Steps
To a solution of 2-(2-methylguanidino)-4-(3-aminocyclohexyl)thiazole (0.5 g.) in methanol (15 ml.) was added dimethyl(cyanoimido)dithiocarbonate (0.3 g.) and the resulting solution allowed to stand at room temperature overnight. Concentration of the reaction mixture gave 2-(2-methylguanidino)-4-[3-(3-cyano-2-methylisothioureido)cyclohexyl]thiazole, m.p. 200°-204° (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04342765 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-f7c602eb40e2463696c6ee4f002537ad |
| Source note | uspto-grants-1982_08 |