HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl chloroformate → N-(1-Methyldecyl)-3-phenyl-3-(3-nitrophenyl)propenamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl chloroformate | HCID 10928 | — |
| Reactant | 2-Undecanamine | HCID 114476 | — |
| Reactant | 3-Phenyl-3-(3-nitrophenyl)propenoic acid | HCID 53686424 | — |
| Product | N-(1-Methyldecyl)-3-phenyl-3-(3-nitrophenyl)propenamide | HCID 53762315 | — |
Reaction Steps
The title compound was prepared from 3-phenyl-3-(3-nitrophenyl)propenoic acid via mixed anhydride formation using ethyl chloroformate, followed by reaction with 1-methyldecylamine, substantially according to the procedure of Preparation 21. This gave a 92% yield of an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04342781 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-e4f5ef47918d4acabaa25bcfb67f94e6 |
| Source note | uspto-grants-1982_08 |