反应详情

温度

130 °C

When all of the water of the reaction has been eliminated, 55 g of tris(2-chloroethyl)amine hydrochloride are introduced. The mixture is heated at 130° C. for 5 hours, then cooled. Excess sodium alcoholate is then neutralized with a 10% aqueous solution of hydrochloric acid. The 3-oxaheptan-1-ol is removed by distillation and the sodium chloride is removed by filtration. The desired product, tris(3,6-dioxadecyl)amine, is distilled (192° C. under 0.1 mmHg).

1. temperaturecooled
2. customThe 3-oxaheptan-1-ol is removed by distillation
3. customthe sodium chloride is removed by filtration
4. distillationThe desired product, tris(3,6-dioxadecyl)amine, is distilled (192° C. under 0.1 mmHg)