HuagongsheHuagongshe Chemistry Print Report · For research reference only
Itaconic acid → Trans-N-[1-Methyldecyl]-2-[4-(4-carboxy-2-oxo-pyrrolidino)phenyl]cyclopropanecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Itaconic acid | HCID 811 | — |
| Reactant | trans-N-(1-Methyldecyl)-2-(4-aminophenyl)cyclopropanecarboxamide | HCID 54155861 | — |
| Product | Trans-N-[1-Methyldecyl]-2-[4-(4-carboxy-2-oxo-pyrrolidino)phenyl]cyclopropanecarboxamide | HCID 54373403 | — |
Reaction Steps
The title compound was prepared from trans-N-(1-methyldecyl)-2-(4-aminophenyl)cyclopropanecarboxamide and itaconic acid, substantially according to the procedure of Example 10. It was recrystallized from acetic acid to give a 21% yield of material having a melting point of 226°-228° C. The infrared spectrum (KBr disc) showed absorptions at 3280, 2900, 1695 and 1625 cm-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04343813 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-ebe85227a196450bac8b8b824144c40a |
| Source note | uspto-grants-1982_08 |