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HRID66801

反应详情

EQUATION

反应方程式

HRID 66801 的结构方程式

REACTANTS

反应物

2
结构：C=C(CC(=O)O)C(=O)O
HCID811

Methylenebutanedioic acid

C5H6O4

结构：CCCCCCCCCC(C)NC(=O)[C@@H]1C[C@H]1c1ccc(N)cc1
HCID54155861

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCC(C)NC(=O)[C@@H]1C[C@H]1c1ccc(N2CC(C(=O)O)CC2=O)cc1
HCID54373403

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from trans-N-(1-methyldecyl)-2-(4-aminophenyl)cyclopropanecarboxamide and itaconic acid, substantially according to the procedure of Example 10. It was recrystallized from acetic acid to give a 21% yield of material having a melting point of 226°-228° C. The infrared spectrum (KBr disc) showed absorptions at 3280, 2900, 1695 and 1625 cm-1.

WORKUP

后处理

  1. customIt was recrystallized from acetic acid