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HRID66803

反应详情

EQUATION

反应方程式

HRID 66803 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc([N+](=O)[O-])cc1
HCID541

4-Nitrobenzaldehyde

C7H5NO3

结构：CCOC(=O)C(C)=P(c1ccccc1)(c1ccccc1)c1ccccc1
HCID79792

Ethyl 2-(triphenylphosphoranylidene)propionate

C23H23O2P

PRODUCTS

生成物

1
结构：CCOC(=O)C(C)=Cc1ccc([N+](=O)[O-])cc1
HCID54080096

Ethyl 2-methyl-3-(4-nitrophenyl)prop-2-enoate

C12H13NO4

收率 56%

PROCEDURE

实验过程

The title compound was prepared from triphenyl(1-[ethoxycarbonyl]ethylidene)phosphorane and 4-nitrobenzaldehyde, substantially according to Preparation 5. The product was obtained in 56% yield, as an orange-yellow solid, m.p. 70.5°-73° C.

WORKUP

后处理

  1. customsubstantially according to Preparation 5
  2. customThe product was obtained in 56% yield, as an orange-yellow solid, m.p. 70.5°-73° C.