HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(1-Methyldecyl)-3-(3-Nitrophenyl)-2-butenamide → HCID 54502184, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(1-Methyldecyl)-3-(3-Nitrophenyl)-2-butenamide | HCID 53905448 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 54502184 | HCID 54502184 | — |
Reaction Steps
The N-(1-methyldecyl)-3-(3-nitrophenyl)-2-butenamide from Preparation 23 (6.5 g.) was reduced with iron powder (5.0 g.) in glacial acetic acid (80 ml.) in a manner analogously to Preparation 27. After chromatography, 4.5 g. of the title compound was obtained, as an amber oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04343813 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-d96bdb1a6b4e4da1912ceaee73b6dc48 |
| Source note | uspto-grants-1982_08 |