Hydrochloric Acid → HCID 70548639, compound

HRID 66888Notes

Reaction equation

HRID 66888 reaction equation
C([O:3][C:4](=[O:28])[C:5]([CH3:27])([O:7][C:8]1[CH:9]=[C:10]2[C:14](=[CH:15][CH:16]=1)[N:13]([CH2:17][CH2:18][CH3:19])[C:12]([C:20]1[CH:25]=[CH:24][N:23]=[CH:22][CH:21]=1)=[C:11]2[CH3:26])[CH3:6])C.[ClH:29]>>[ClH:29].[CH3:6][C:5]([O:7][C:8]1[CH:9]=[C:10]2[C:14](=[CH:15][CH:16]=1)[N:13]([CH2:17][CH2:18][CH3:19])[C:12]([C:20]1[CH:25]=[CH:24][N:23]=[CH:22][CH:21]=1)=[C:11]2[CH3:26])([CH3:27])[C:4]([OH:28])=[O:3]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 538957452-methyl-2-[3-methyl-1-propyl-2-(4-pyridyl)-1H-indole-5-yloxy]propanoic acid ethylester

Product 1

HCID 70548639HCID 70548639, compound

Procedure

The above compound was prepared from 2-methyl-2-[3-methyl-1-propyl-2-(4-pyridyl)-1H-indole-5-yloxy]propanoic acid ethylester by hydrolysis with diluted hydrochloric acid at the boiling temperature. After the hydrochloric acid was distilled off in vacuo, the reaction product was recrystallized from acetone.

Workup

  1. distillationAfter the hydrochloric acid was distilled off in vacuo
  2. customthe reaction product was recrystallized from acetone

Sources & evidence

ORD record
ord-406739993b464f6e85a11eda7de205f7
Source dataset
uspto-grants-1982_08
Patent number
US04343811

Reaction notes

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