反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
In a process for purifying crude molten 2-mercaptobenzothiazole, prepared by reacting aniline carbon disulfide and sulfur at elevated temperature and pressure, in which the purification includes the steps of separating dissolved alkali metal salt of 2-mercaptobenzothiazole from undissolved impurities, treating the dissolved alkali metal salt of 2-mercaptobenzothiazole with an excess of a non-oxidizing mineral acid to precipitate a slurry of purified 2-mercaptobenzothiazole, separating the purified 2-mercaptobenzothiazole solids from the slurry to obtain 2-mercaptobenzothiazole solids, washing the solids with water, and drying the purified 2-mercaptobenzothiazole, the improvement comprising; forming said dissolved alkali metal salt at 2-mercaptobenzothiazole and said dissolved impurities by the steps of
WORKUP
后处理
- customIn a process for purifying crude molten 2-mercaptobenzothiazole
- customprepared
- customin which the purification
- customof separating
- dissolutiondissolved alkali metal salt of 2-mercaptobenzothiazole from undissolved impurities
- additiontreating the dissolved alkali metal salt of 2-mercaptobenzothiazole with an excess of a non-oxidizing mineral acid
- customto precipitate a slurry of purified 2-mercaptobenzothiazole
- customseparating the purified 2-mercaptobenzothiazole solids from the slurry