HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 12797987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | 1-(3,4-methylenedioxybenzoylmethyl)-4-[3,4-dihydro-2(1H)-quinazolinon-3-yl]-piperidine | HCID 12797985 | — |
| Product | HCID 12797987 | HCID 12797987 | 67.8% |
Reaction Steps
In this example, the procedure of Example 3 is repeated except that 2.2 g of 1-(3,4-methylenedioxybenzoylmethyl)-4-[3,4-dihydro-2(1H)-quinazolinon-3-yl]-piperidine and 410 mg of sodium borohydride are used to obtain 1.69 g of a crude product. The crude product is recrystallized from hot ethanol to obtain 1.50 g of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04344948 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-60febbc6e4eb4d87bff29adb7f125753 |
| Source note | uspto-grants-1982_08 |