huagongshe.com
HRID67122

反应详情

EQUATION

反应方程式

HRID 67122 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CC1(C)C(C=C(Br)Br)C1C(=O)Cl
HCID12940582

3-(2,2-Dibromoethenyl)-2,2-dimethylcyclopropane-1-carbonyl chloride

C8H9Br2ClO

结构：C=CC(O)c1cccc(Oc2ccccc2)c1
HCID12961393

未命名化合物

PRODUCTS

生成物

1
结构：C=CC(OC(=O)C1C(C=C(Br)Br)C1(C)C)c1cccc(Oc2ccccc2)c1
HCID12855381

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

15.8 g (0.05 mole) of 2,2-dimethyl-3-(2',2'-dibromovinyl)-cyclopropanecarboxylic acid chloride are added dropwise, whilst stirring, to 5.1 g (0.05 mole) of pyridine, 100 ml of absolute ether and 11.4 g (0.05 mole) of 3-phenoxy-α-vinyl-benzyl alcohol at 0°-5° C.