HRID67642

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID69194

1-Isocyanato-2-methylbenzene

C8H7NO

HCID178429390

未命名化合物

PRODUCTS

生成物

HCID178424380

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID7237

o-Xylene

C8H10

PROCEDURE

实验过程

A mixture of 22.4 g (0.2 mol) 5-hydroxy-1,3-dimethyl-1H-pyrazole [K. Auwers, J.Prakt.Chem., 110, 153 (1925)], 26.6 g (0.2 mol) o-tolylisocyanate in 150 ml xylene containing 1 ml triethylamine is heated to reflux for 1.5 hours.

WORKUP

后处理

temperatureis heated
temperatureto reflux for 1.5 hours