HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 4-dodecoxyethylaminoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | N-dodecoxyethyldiethylenetriamine | HCID 20527003 | — |
| Product | 4-dodecoxyethylaminoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one | HCID 70548316 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 315.1 g (1 mole) of N-dodecoxyethyldiethylenetriamine and 130.1 g (1 mole) of ethyl acetoacetate at 150° to 160° C., 18 g of water and 46 g of ethanol were distilled off to obtain 4-dodecoxyethylaminoethyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-338dd568fcad46b7afde5f9a9ad1621f |
| Source note | uspto-grants-1982_08 |