HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 54347639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | N-octoxypropylethylenediamine | HCID 57223339 | — |
| Product | HCID 54347639 | HCID 54347639 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 230.1 g (1 mole) of N-octoxypropylethylenediamine and 116.1 g (1 mole) of methyl acetoacetate. At 140° to 145° C., 18 g of water and 32 g of ethanol were distilled off to obtain 4-octoxypropyl-7-methyl-3,6-dihydro-2H-1,4-diazepin-5-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-b1e702d1ee1e4121a901cc5708ca2c82 |
| Source note | uspto-grants-1982_08 |