Butyl 3-formylpropionate → HCID 54181441, compound

HRID 67680Notes

Reaction equation

HRID 67680 reaction equation
[CH2:1]([NH:19][CH2:20][CH2:21][NH2:22])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH:23]([CH2:25][CH2:26][C:27](OCCCC)=O)=[O:24]>>[CH2:1]([N:19]1[C:23](=[O:24])[CH2:25][CH2:26][CH:27]=[N:22][CH2:21][CH2:20]1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH:9]=[CH:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

3

Reactant 2

HCID 13587906Butyl 3-formylpropionateHCID 53754734N~1~-(Octadec-9-en-1-yl)ethane-1,2-diamine

Product 1

HCID 54181441HCID 54181441, compound

Procedure

Into an apparatus similar to that in Example 1, were charged 310.1 g (1 mole) of N-(9-octadecenyl)ethylenediamine and 158.2 g (1 mole) of butyl 3-formylpropionate. At 150° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off to obtain 4-(9-octadecenyl)-2,3,6,7-tetrahydro-1,4-diazocin-5-one.

Workup

  1. distillationAt 150° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off

Sources & evidence

ORD record
ord-3c57406900944b08a9509c69ca742124
Source dataset
uspto-grants-1982_08
Patent number
US04346087

Reaction notes

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