HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl 3-formylpropionate → HCID 54181441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl 3-formylpropionate | HCID 13587906 | — |
| Reactant | N~1~-(Octadec-9-en-1-yl)ethane-1,2-diamine | HCID 53754734 | — |
| Product | HCID 54181441 | HCID 54181441 | — |
Reaction Steps
Into an apparatus similar to that in Example 1, were charged 310.1 g (1 mole) of N-(9-octadecenyl)ethylenediamine and 158.2 g (1 mole) of butyl 3-formylpropionate. At 150° C. and under a reduced pressure of 50 mmHg, 18 g of water and 74 g of butanol were distilled off to obtain 4-(9-octadecenyl)-2,3,6,7-tetrahydro-1,4-diazocin-5-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346087 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-3c57406900944b08a9509c69ca742124 |
| Source note | uspto-grants-1982_08 |