HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 7196680, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 4-Amino-6-methyl-3-sulfanyl-4,5-dihydro-1,2,4-triazin-5-one | HCID 1284234 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 7196680 | HCID 7196680 | — |
Reaction Steps
6.5 Parts by weight of 4-amino-2,3-dihydro-6-methyl-3-thiono-as-triazin-5(4H)-one is added to a solution of 2.3 parts by weight of sodium methoxide in 50 parts by volume of methanol. After a few minutes 5.2 parts by weight of benzylchloride is added and the resulting mixture is stirred over night at room temperature. The solvent is removed under vacuum and the residue is washed with water to give 4.5 parts of 4-amino-3-benzylthio-6-methyl-as-triazin-5(4H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346220 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-b92e151b05bc447282cdf60f817cd47a |
| Source note | uspto-grants-1982_08 |