HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propanal → HCID 178438255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propanal | HCID 527 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178438255 | HCID 178438255 | — |
Reaction Steps
A 10.5 g. portion of 4-methylthiosemicarbazide was reacted with 5.8 g. of propionaldehyde in the presence of 7.9 g. of pyridine and 200 ml. of toluene, and 12.1 g. of pivaloyl chloride was added to produce 13.8 g. of the desired product, m.p. 78.5°-80°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346225 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-ba8d6bf00d254426b30add6720239cc1 |
| Source note | uspto-grants-1982_08 |