HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 178482499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 2-Fluorobenzoyl chloride | HCID 9808 | — |
| Reactant | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 178482499 | HCID 178482499 | — |
Reaction Steps
A 42 g. portion of 4-methylthiosemicarbazide was reacted with 400 ml. of acetone, and then with 32 ml. of pyridine and 63.6 g. of 2-fluorobenzoyl chloride to prepare 66.5 g. of the desired product, m.p. 136°-140°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346225 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-942626b67a8a4711bd9a19d156dd0fc4 |
| Source note | uspto-grants-1982_08 |