huagongshe.com
HRID67746

反应详情

EQUATION

反应方程式

HRID 67746 的结构方程式

REACTANTS

反应物

1
结构：CN1C(=Nc2ccccc2)SCC1(O)c1ccc(Cl)c(S(=O)(=O)N(C)C)c1
HCID20527326

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)S(=O)(=O)c1cc(-c2csc(=Nc3ccccc3)n2C)ccc1Cl
HCID3047726

Metibride

C18H18ClN3O2S2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

8.52 g (0.02 mole) of 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-phenyliminothiazolidin-4-ol in 100 ml of glacial acetic acid are heated at the boil for 3 hours, the solvent is distilled off and the residue is made to crystallize using water. Melting point 180° C.

WORKUP

后处理

  1. distillationthe solvent is distilled off
  2. customto crystallize