HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-phenyliminothiazolidin-4-ol → Metibride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-phenyliminothiazolidin-4-ol | HCID 20527326 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Metibride | HCID 3047726 | — |
Reaction Steps
8.52 g (0.02 mole) of 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-phenyliminothiazolidin-4-ol in 100 ml of glacial acetic acid are heated at the boil for 3 hours, the solvent is distilled off and the residue is made to crystallize using water. Melting point 180° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346088 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-2c83853343d54aa4bb66be59f786f2ba |
| Source note | uspto-grants-1982_08 |