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HRID67747

反应详情

EQUATION

反应方程式

HRID 67747 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CN(C)S(=O)(=O)c1cc(-c2csc(=Nc3ccccc3)n2C)ccc1Cl
HCID3047726

Metibride

C18H18ClN3O2S2

PRODUCTS

生成物

1
结构：CN(C)S(=O)(=O)c1cc(-c2csc(=Nc3ccccc3)n2C)ccc1Cl.Cl
HCID20527457

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

8.9 g (0.02 mole) of 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-phenylimino-4-thiazoline in 150 ml of methanol are acidified with a saturated ethereal solution of hydrogen chloride, the solvent is distilled off and the residue is recrystallized from ethanol. Melting point 229°-233° C. (with decomposition).

WORKUP

后处理

  1. distillationthe solvent is distilled off
  2. customthe residue is recrystallized from ethanol