Triethylamine → HCID 20527096, compound

HRID 67750Notes

Reaction equation

HRID 67750 reaction equation
Br.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]([CH3:22])[C:11](=[N:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[CH3:21])[S:12][CH:13]=2)=[CH:5][C:4]=1[S:23](=[O:28])(=[O:27])[N:24]([CH3:26])[CH3:25].C(N(CC)CC)C.CO.C(OCC)(=O)C>CO>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]([CH3:22])[C:11](=[N:14][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=3[CH3:21])[S:12][CH:13]=2)=[CH:5][C:4]=1[S:23](=[O:28])(=[O:27])[N:24]([CH3:26])[CH3:25]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 205270954-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2-methylphenylimino)-4-thiazoline hydrobromideHCID 21584119Ethylacetate methanol

Product 1

HCID 20527096HCID 20527096, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2-methylphenylimino)-4-thiazoline hydrobromide with triethylamine in methanol. Colorless crystals from methanol/ethyl acetate; melting point 158°-162° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-662ec38394164760afae35d5ff44ac25
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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