Triethylamine → 2-(4-Diethylaminophenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline

HRID 67752Notes

Reaction equation

HRID 67752 reaction equation
Br.[CH2:2]([N:4]([CH2:31][CH3:32])[C:5]1[CH:10]=[CH:9][C:8]([N:11]=[C:12]2[N:16]([CH3:17])[C:15]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[C:20]([S:25](=[O:30])(=[O:29])[N:26]([CH3:28])[CH3:27])[CH:19]=3)=[CH:14][S:13]2)=[CH:7][CH:6]=1)[CH3:3].C(N(CC)CC)C>CO>[CH2:31]([N:4]([CH2:2][CH3:3])[C:5]1[CH:6]=[CH:7][C:8]([N:11]=[C:12]2[N:16]([CH3:17])[C:15]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[C:20]([S:25](=[O:29])(=[O:30])[N:26]([CH3:27])[CH3:28])[CH:19]=3)=[CH:14][S:13]2)=[CH:9][CH:10]=1)[CH3:32]

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 205271652-(4-Diethylaminophenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide

Product 1

HCID 205271662-(4-Diethylaminophenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from 2-(4-diethylaminophenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide and triethylamine in methanol at room temperature. Melting point 184°-185° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-739616652ab94a4e848c72210d67da0f
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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