Triethylamine → 4-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2,3-dimethylphenyl-imino)-4-thiazoline

HRID 67760Notes

Reaction equation

HRID 67760 reaction equation
Br.[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]([CH3:23])[C:11](=[N:14][C:15]3[CH:20]=[CH:19][CH:18]=[C:17]([CH3:21])[C:16]=3[CH3:22])[S:12][CH:13]=2)=[CH:5][C:4]=1[S:24](=[O:29])(=[O:28])[N:25]([CH3:27])[CH3:26].C(N(CC)CC)C>CO>[Cl:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[N:10]([CH3:23])[C:11](=[N:14][C:15]3[CH:20]=[CH:19][CH:18]=[C:17]([CH3:21])[C:16]=3[CH3:22])[S:12][CH:13]=2)=[CH:5][C:4]=1[S:24](=[O:29])(=[O:28])[N:25]([CH3:27])[CH3:26]

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 20527370HCID 20527370, compound

Product 1

HCID 205273714-(4-Chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2,3-dimethylphenyl-imino)-4-thiazoline

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from 4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-2-(2,3-dimethylphenyl-imino)-4-thiazoline hydrobromide and triethylamine in methanol. Melting point 226° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-13b0ad4a710143c4a09a2d03b32a3bac
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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