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HRID67761

反应详情

EQUATION

反应方程式

HRID 67761 的结构方程式

REACTANTS

反应物

1
结构：Br.Cc1c(Cl)cccc1N=C1SCC(O)(c2ccc(Cl)c(S(=O)(=O)N(C)C)c2)N1C
HCID70532717

未命名化合物

PRODUCTS

生成物

1
结构：Br.Cc1c(Cl)cccc1N=c1scc(-c2ccc(Cl)c(S(=O)(=O)N(C)C)c2)n1C
HCID20527315

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

结构：CCC(=O)O
溶剂HCID1032

未命名化合物

PROCEDURE

实验过程

Obtained by a procedure analogous to that indicated in Example 1 (b), from 2-(3-chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methylthiazolidin-4-ol hydrobromide, by heating under reflux for 20 minutes in glacial acetic acid or by heating at 110° C. in propionic acid for 45 minutes. Colorless crystals; melting point 226°-228° C. (with decomposition).

WORKUP

后处理

  1. customObtained by a procedure analogous to
  2. temperatureby heating