HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70532717, compound → 2-(3-Chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70532717 | HCID 70532717 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Propionic Acid | HCID 1032 | — |
| Product | 2-(3-Chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide | HCID 20527315 | — |
Reaction Steps
Obtained by a procedure analogous to that indicated in Example 1 (b), from 2-(3-chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methylthiazolidin-4-ol hydrobromide, by heating under reflux for 20 minutes in glacial acetic acid or by heating at 110° C. in propionic acid for 45 minutes. Colorless crystals; melting point 226°-228° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346088 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-eafbe7d8182f4771ba79c286f60aa5cc |
| Source note | uspto-grants-1982_08 |