Ammonia → HCID 20527249, compound

HRID 67762Notes

Reaction equation

HRID 67762 reaction equation
Br.[Cl:2][C:3]1[C:4]([CH3:29])=[C:5]([N:9]=[C:10]2[N:14]([CH3:15])[C:13]([C:16]3[CH:21]=[CH:20][C:19]([Cl:22])=[C:18]([S:23](=[O:28])(=[O:27])[N:24]([CH3:26])[CH3:25])[CH:17]=3)=[CH:12][S:11]2)[CH:6]=[CH:7][CH:8]=1.N>C(N(CC)CC)C>[Cl:2][C:3]1[C:4]([CH3:29])=[C:5]([N:9]=[C:10]2[N:14]([CH3:15])[C:13]([C:16]3[CH:21]=[CH:20][C:19]([Cl:22])=[C:18]([S:23](=[O:28])(=[O:27])[N:24]([CH3:25])[CH3:26])[CH:17]=3)=[CH:12][S:11]2)[CH:6]=[CH:7][CH:8]=1

Participants

4

Reactant 2

HCID 222AmmoniaHCID 205273152-(3-Chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide

Product 1

HCID 20527249HCID 20527249, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Obtained by a procedure analogous to that indicated in Example 2 (a), from 2-(3-chloro-2-methylphenyl-imino)-4-(4-chloro-3-dimethylsulfamoylphenyl)-3-methyl-4-thiazoline hydrobromide, the reaction mixture being rendered alkaline with a 20% methanolic ammonia solution instead of with triethylamine and worked up as in Example 2 (a). Colorless crystals; melting point 144°-146° C.

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-3c1f844b77d04ab4b57b4e47f364af50
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

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