Thiourea, N-(1-methylpropyl)-N'-phenyl- → 3-sec.-Butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenylimino-4-thiazoline hydrobromide

HRID 67765Notes

Reaction equation

HRID 67765 reaction equation
[Br:1]CC(C1C=CC(Cl)=C(S(=O)(=O)N(C)C)C=1)=O.C(NC(=S)NC1C=CC=CC=1)(CC)C.Br.[CH:33]([N:37]1[C:41]([C:43]2[CH:48]=[CH:47][C:46]([Cl:49])=[C:45]([S:50](=[O:55])(=[O:54])[N:51]([CH3:53])[CH3:52])[CH:44]=2)(O)[CH2:40][S:39][C:38]1=[N:56][C:57]1[CH:62]=[CH:61][CH:60]=[CH:59][CH:58]=1)([CH2:35][CH3:36])[CH3:34]>>[BrH:1].[CH:33]([N:37]1[C:41]([C:43]2[CH:48]=[CH:47][C:46]([Cl:49])=[C:45]([S:50](=[O:54])(=[O:55])[N:51]([CH3:53])[CH3:52])[CH:44]=2)=[CH:40][S:39][C:38]1=[N:56][C:57]1[CH:62]=[CH:61][CH:60]=[CH:59][CH:58]=1)([CH2:35][CH3:36])[CH3:34]

Participants

4

Reactant 3

HCID 2826863Thiourea, N-(1-methylpropyl)-N'-phenyl-HCID 204768462-Bromo-4'-chloro-3'-dimethylsulfamoylacetophenoneHCID 20527413HCID 20527413, compound

Product 1

HCID 205273803-sec.-Butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenylimino-4-thiazoline hydrobromide

Procedure

Obtained by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-sec.-butyl-1-phenylthiourea, or by a procedure analogous to that of Example 1(b), from 3-sec.-butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 250° C. (with decomposition).

Workup

  1. customObtained by a procedure analogous to

Sources & evidence

ORD record
ord-4f5bb257850548228392262acd3f3eb7
Source dataset
uspto-grants-1982_08
Patent number
US04346088

Reaction notes

Loading…