HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea, N-(1-methylpropyl)-N'-phenyl- → 3-sec.-Butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenylimino-4-thiazoline hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea, N-(1-methylpropyl)-N'-phenyl- | HCID 2826863 | — |
| Reactant | 2-Bromo-4'-chloro-3'-dimethylsulfamoylacetophenone | HCID 20476846 | — |
| Reactant | HCID 20527413 | HCID 20527413 | — |
| Product | 3-sec.-Butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenylimino-4-thiazoline hydrobromide | HCID 20527380 | — |
Reaction Steps
Obtained by a procedure analogous to that indicated in Example 1(a), from 2-bromo-4'-chloro-3'-dimethylsulfamoylacetophenone and 3-sec.-butyl-1-phenylthiourea, or by a procedure analogous to that of Example 1(b), from 3-sec.-butyl-4-(4-chloro-3-dimethylsulfamoylphenyl)-2-phenyliminothiazolidin-4-ol hydrobromide. Colorless crystals; melting point 250° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346088 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-4f5bb257850548228392262acd3f3eb7 |
| Source note | uspto-grants-1982_08 |