Hydrogen Bromide → HCID 20527232, compound

HRID 67772Notes

Reaction equation

Br.Br.[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:24])[C:12](=[N:15][C:16]3[CH:21]=[CH:20][CH:19]=[C:18]([CH3:22])[C:17]=3[CH3:23])[S:13][CH:14]=2)=[CH:6][C:5]=1[S:25](=[O:34])(=[O:33])[N:26]([CH2:30][CH2:31][CH3:32])[CH2:27][CH2:28][CH3:29]>>[Cl:3][C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:11]([CH3:24])[C:12](=[N:15][C:16]3[CH:21]=[CH:20][CH:19]=[C:18]([CH3:22])[C:17]=3[CH3:23])[S:13][CH:14]=2)=[CH:6][C:5]=1[S:25](=[O:34])(=[O:33])[N:26]([CH2:27][CH2:28][CH3:29])[CH2:30][CH2:31][CH3:32]

Participants

Reactant 2

HCID 260Hydrogen Bromide

HCID 20527307HCID 20527307, compound

Product 1

HCID 20527232HCID 20527232, compound

Procedure

Obtained by a procedure analogous to that indicated in Example 2(a), from the hydrobromide of the title compound (Example 61). Colorless crystals; melting point 184°-187° C.

Workup

customObtained by a procedure analogous to

Sources & evidence

ORD record: ord-330a7c40a9bd456498c7fb39fbe6d8eb
Source dataset: uspto-grants-1982_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04346088

Reaction notes

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