HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 20527426, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | 4-(4-Chloro-3-sulfamoylphenyl)-3-methyl-2-(4-methylphenyl-imino)-thiazolidin-4-ol hydrobromide | HCID 70553549 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20527426 | HCID 20527426 | — |
Reaction Steps
0.02 mole (9.8 g) of 4-(4-chloro-3-sulfamoylphenyl)-3-methyl-2-(4-methylphenyl-imino)-thiazolidin-4-ol hydrobromide are boiled in 120 ml of ethanol for 2 hours under reflux. After cooling to room temperature, 200 ml of diisopropyl ether are added and the crystals are filtered off. Melting point 265° C. (with decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346088 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-3e3fc435b5a748fdb25a38e297db18be |
| Source note | uspto-grants-1982_08 |