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HRID67775

反应详情

EQUATION

反应方程式

HRID 67775 的结构方程式

REACTANTS

反应物

2
结构：CC(C)OC(C)C
HCID7914

Isopropyl ether

C6H14O

结构：Br.Cc1ccc(N=C2SCC(O)(c3ccc(Cl)c(S(N)(=O)=O)c3)N2C)cc1
HCID70553549

未命名化合物

PRODUCTS

生成物

1
结构：Br.Cc1ccc(N=c2scc(-c3ccc(Cl)c(S(N)(=O)=O)c3)n2C)cc1
HCID20527426

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

0.02 mole (9.8 g) of 4-(4-chloro-3-sulfamoylphenyl)-3-methyl-2-(4-methylphenyl-imino)-thiazolidin-4-ol hydrobromide are boiled in 120 ml of ethanol for 2 hours under reflux. After cooling to room temperature, 200 ml of diisopropyl ether are added and the crystals are filtered off. Melting point 265° C. (with decomposition).

WORKUP

后处理

  1. temperatureunder reflux
  2. filtrationthe crystals are filtered off