HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20476837, compound → 2-Bromo-3'-methyl-5'-sulfamoylacetophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20476837 | HCID 20476837 | — |
| Reactant | 2-Bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone | HCID 20476841 | — |
| Reactant | 2-Bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone | HCID 20527157 | — |
| Reactant | 2-Bromo-2'-chloro-5'-sulfamoylacetophenone | HCID 20527308 | — |
| Reactant | HCID 20527387 | HCID 20527387 | — |
| Reactant | HCID 20527402 | HCID 20527402 | — |
| Reactant | HCID 20527440 | HCID 20527440 | — |
| Reactant | HCID 20527473 | HCID 20527473 | — |
| Product | 2-Bromo-3'-methyl-5'-sulfamoylacetophenone | HCID 20527134 | — |
Reaction Steps
The bromoacetophenones listed below were prepared in an analogous manner: 2,2'-dibromo-5'-dimethylsulfamoyl-acetophenone, melting point 88° C., 2-bromo-3'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 77°-78° C., 2-bromo-2'-chloro-5'-methylsulfamoyl-acetophenone, melting point 99°-101° C., 2-bromo-2'-chloro-5'-dimethylsulfamoyl-acetophenone, melting point 87°-88° C., 2-bromo-2'-chloro-5'-sulfamoylacetophenone, melting point 152°-154° C., 2-bromo-3'-methyl-5'-dimethylsulfamoylacetophenone, melting point 71°-75° C., 2-bromo-2'-methyl-5'-dimethylsulfamoylacetophenone, melting point 69°-71° C. and 2-bromo-2'-methyl-5'-sulfamoylacetophenone, melting point 112°-115° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04346088 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-e9deda43a70e4259ab4aa93b071fa763 |
| Source note | uspto-grants-1982_08 |