Sarcosine → HCID 53992343, compound

HRID 67793Notes

Reaction equation

[NH:1]([CH2:3][C:4](O)=O)[CH3:2].[OH-:7].[Na+].Cl[NH:10][C:11](=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>O>[CH2:3]([NH:1][C:2]([NH:10][C:11](=[O:23])[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])=[O:7])[CH2:4][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

Conditions

Temperature: 50 °C

Procedure

A solution of 8.9 g (0.1 mol) of sarcosine and 8 g (0.2 mol) of sodium hydroxide in 40 ml of water was added to a suspension of 23.35 g (0.1 mol) of lauric N-chloramide in 200 ml of water. While the reaction mixture was heated to 50° C., acyl urea separates from the suspension in the form of flocks and was isolated by filtration to yield 17 g (86% yield) of N-n-undecyl-N'-lauroyl urea of the formula ##STR19## having a melting point of 104°-106° C. 105° C.; 108° C.; (literature: Jefreys, Am. 22, 33; Ehestaedt, thesis (Freiburg i.B., 1886) p. 15).

Workup

customwas isolated by filtration

Sources & evidence

ORD record: ord-3f4715205ce148c09a6ae8324377f9e4
Source dataset: uspto-grants-1982_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04346233

Reaction notes

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