Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sarcosine | HCID 1088 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | lauric N-chloramide | HCID 19040106 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 53992343 | HCID 53992343 | 86% |
Reaction Steps
A solution of 8.9 g (0.1 mol) of sarcosine and 8 g (0.2 mol) of sodium hydroxide in 40 ml of water was added to a suspension of 23.35 g (0.1 mol) of lauric N-chloramide in 200 ml of water. While the reaction mixture was heated to 50° C., acyl urea separates from the suspension in the form of flocks and was isolated by filtration to yield 17 g (86% yield) of N-n-undecyl-N'-lauroyl urea of the formula ##STR19## having a melting point of 104°-106° C. 105° C.; 108° C.; (literature: Jefreys, Am. 22, 33; Ehestaedt, thesis (Freiburg i.B., 1886) p. 15).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04346233 |
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| Source dataset | uspto-grants-1982_08 |
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| ORD ID | ord-3f4715205ce148c09a6ae8324377f9e4 |
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| Source note | uspto-grants-1982_08 |
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