HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-Acetylthio-3-chlorobenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Chloro-2-mercaptobenzoic acid | HCID 13162400 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Acetylthio-3-chlorobenzoic acid | HCID 13420405 | — |
Reaction Steps
3-Chloro-2-mercaptobenzoic acid (9.8 g, 52 mmol), acetic anhydride (6.3 g, 62 mmol) and glacial acetic acid (22 ml) were heated at 80° C. for 4 hours, then cooled and mixed with dilute hydrochloric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04347246 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-04a985bfd36648db9ebe8342f700336d |
| Source note | uspto-grants-1982_08 |