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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 6801Generated: October 28, 2026

HCID 69593882, compound → HCID 22018869, compound

https://huagongshe.com/reaction/6801

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69593882HCID 69593882—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 22018869HCID 22018869—

Reaction Steps

The product of Step C (2.2 g, 8.1 mmol) in 40 mL methanol and 5% palladium on carbon (0.25 g) was stirred under hydrogen atmosphere (balloon) for 1 h. The reaction mixture was filtered through filter aid and the solvent removed under vacuum to afford the product as a solid, MS: m/z 276 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07084156B2
Source datasetuspto-grants-2006_08
ORD IDord-88fe29ea69b54e5088b5bb28e789c315
Source noteuspto-grants-2006_08