HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69593882, compound → HCID 22018869, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69593882 | HCID 69593882 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22018869 | HCID 22018869 | — |
Reaction Steps
The product of Step C (2.2 g, 8.1 mmol) in 40 mL methanol and 5% palladium on carbon (0.25 g) was stirred under hydrogen atmosphere (balloon) for 1 h. The reaction mixture was filtered through filter aid and the solvent removed under vacuum to afford the product as a solid, MS: m/z 276 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07084156B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-88fe29ea69b54e5088b5bb28e789c315 |
| Source note | uspto-grants-2006_08 |