HRID68012

反应详情

EQUATION

反应方程式

HRID 68012 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

154 g (1 mole) of 3,6-dimethyl-oct-1-yn-3ol are dissolved in 100 ml of methanol, 1 g of an 0.1% strength palladium/calcium carbonate catalyst, which has been poisoned with zinc ions, is added, and hydrogen is passed in at 20° C. under atmospheric pressure. The hydrogenation is complete in 6 hours, when about 24 liters of hydrogen have been absorbed.

WORKUP

后处理

  1. additionis added
  2. customis passed in at 20° C. under atmospheric pressure
  3. customwhen about 24 liters of hydrogen have been absorbed