HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Octyn-3-ol, 3,6-dimethyl- → 3,6-Dimethyl-oct-1-en-3-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Octyn-3-ol, 3,6-dimethyl- | HCID 174244 | — |
| Edukt | HCID 178418361 | HCID 178418361 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Katalysator | Zinc | HCID 23994 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 3,6-Dimethyl-oct-1-en-3-ol | HCID 20526739 | — |
Reaktionsschritte
154 g (1 mole) of 3,6-dimethyl-oct-1-yn-3ol are dissolved in 100 ml of methanol, 1 g of an 0.1% strength palladium/calcium carbonate catalyst, which has been poisoned with zinc ions, is added, and hydrogen is passed in at 20° C. under atmospheric pressure. The hydrogenation is complete in 6 hours, when about 24 liters of hydrogen have been absorbed.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04347388 |
| Quelldatensatz | uspto-grants-1982_08 |
| ORD ID | ord-a7393b65dacd4364838b740a4c2e917c |
| Quellennotiz | uspto-grants-1982_08 |