反应详情

Into a 100 mL round bottom flask a mixture of 5 parts of 3-tert-butyldimethylsilyloxybenzoic acid and 25 mL of thionyl chloride was heated at reflux for 1 hr 30 min. The reaction mixture was concentrated under reduced pressure to yield 5.77 parts of an oil.

1. temperaturewas heated
2. temperatureat reflux for 1 hr 30 min
3. concentrationThe reaction mixture was concentrated under reduced pressure
4. customto yield 5.77 parts of an oil