HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86696919, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 15987642 | HCID 15987642 | — |
| Product | HCID 86696919 | HCID 86696919 | 87.5% |
Reaction Steps
Intermediate e (3 g, 0.012 mol) was added to thionyl chloride (10V/W, 30 mL). The mixture was warmed up to react under reflux for 6 h. The solvent was evaporated off to produce a clear yellow crystal (2.8 g) in a yield of 87.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822465B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-3ace713c6dec4862bfafd89796939644 |
| Source note | uspto-grants-2014_09 |