Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 1-(4-Fluoro-3-methyl-phenyl)-3-phenyl-1,3-propanedione | HCID 82120449 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86762669 | HCID 86762669 | — |
Reaction Steps
1.7 g 1-(4-fluoro-3-methyl-phenyl)-3-phenyl-1,3-propanedione was dissolved in 20 mL of a solution of 1 N hydrazine in THF and stirred for 3 h at 75° C. The solvent was removed and the residue was crystallized to give 1.7 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08822464B2 |
|---|
| Source dataset | uspto-grants-2014_09 |
|---|
| ORD ID | ord-8f98da1caea741c3b1546aee72bc285b |
|---|
| Source note | uspto-grants-2014_09 |
|---|
