HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → 4-Cyclopropylamino-3-methyl-piperidine-1-carboxylic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | tert-Butyl 3-methyl-4-oxopiperidine-1-carboxylate | HCID 22644642 | — |
| Product | 4-Cyclopropylamino-3-methyl-piperidine-1-carboxylic acid tert-butyl ester | HCID 68289944 | — |
Reaction Steps
The title compound is prepared from 3-methyl-4-oxo-piperidine-1-carboxylic acid tert-butyl ester and cyclopropylamine following a procedure analogous to that described in Intermediate 7. LC (method 3): tR=1.30 min; Mass spectrum (ESI+): m/z=255 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822471B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-301deab23fa241cbba0c9445cfdc57a8 |
| Source note | uspto-grants-2014_09 |