HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloropyrimidine → HCID 68290045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloropyrimidine | HCID 590641 | — |
| Reactant | HCID 68289916 | HCID 68289916 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 68290045 | HCID 68290045 | — |
Reaction Steps
The title compound is prepared from N-cyclopropyl-4-(4-methyl-oxazol-5-yl)-N-piperidin-4-yl-benzamide trifluoroacetic acid salt and 2,5-dichloro-pyrimidine following a procedure analogous to that described in Example 19 using N-methylpyrrolidinone as solvent. LC (method 6): tR=1.92 min; Mass spectrum (ESI+): m/z=438/440 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822471B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-0206d61a5c8f4c698dd41f9d83e91f0e |
| Source note | uspto-grants-2014_09 |