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HRID69179

反应详情

EQUATION

反应方程式

HRID 69179 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccccc1
HCID6115

Aniline

C6H7N

结构：Nc1cccc(Cl)c1
HCID7932

3-Chloroaniline

C6H6ClN

结构：Clc1cccc(Nc2ccc3ncc(Cc4ccc5ncccc5c4)n3n2)c1
HCID57917421

未命名化合物

PRODUCTS

生成物

1
结构：c1ccc(Nc2ccc3ncc(Cc4ccc5ncccc5c4)n3n2)cc1
HCID57917317

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the compound of Example 121 using aniline as starting material instead of 3-chloroaniline and with a preparative LCMS purification instead of a flash chromatography (tR 4.30 min (conditions 4), MH+=352.3, 1H-NMR in DMSO-d6: 8.91 (m, 1H); 8.36 (m, 1H); 8.17 (d, 1H); 8.08 (s, 1H); 8.03 (d, 1H); 7.96 (m, 1H); 7.79 (m, 1H); 7.58 (dd, 1H); 7.50 (m, 2H); 7.35 (d, 1H); 7.25 (t, 2H); 7.01 (t, 1H); 4.59 (s, 2H)).

WORKUP

后处理

  1. customwith a preparative LCMS purification instead of a flash chromatography (tR 4.30 min (conditions 4), MH+=352.3, 1H-NMR in DMSO-d6: 8.91 (m, 1H); 8.36 (m, 1H); 8.17 (d, 1H); 8.08 (s, 1H); 8.03 (d, 1H); 7.96 (m, 1H); 7.79 (m, 1H); 7.58 (dd, 1H); 7.50 (m, 2H); 7.35 (d, 1H); 7.25 (t, 2H); 7.01 (t, 1H); 4.59 (s, 2H))