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HRID69830

反应详情

EQUATION

反应方程式

HRID 69830 的结构方程式

REACTANTS

反应物

3
结构：CCN(C(C)C)C(C)C
HCID81531

Diisopropylethylamine

C8H19N

结构：CC(C)(C)OC(=O)N[C@H]1CCCNC1
HCID1514171

(S)-3-Boc-aminopiperidine

C10H20N2O2

结构：O=[N+]([O-])c1cnccc1Cl
HCID2735781

4-Chloro-3-nitropyridine

C5H3ClN2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@H]1CCCN(c2ccncc2[N+](=O)[O-])C1
HCID67499955

未命名化合物

收率 99%

PROCEDURE

实验过程

The method of Example 1 was followed using 1 eq each of 4-chloro-3-nitropyridine, (S)-3-N-Boc-amino piperidine and diisopropylethylamine yielding (S)-tert-butyl 1-(3-nitropyridin-4-yl)piperidin-3-ylcarbamate, (99%). LCMS (m/z): 323.1 (MH+); LC Rt=2.13 min.