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HRID69916

反应详情

EQUATION

反应方程式

HRID 69916 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)[Si](C)(C)OC1CCCN(c2ccncc2[N+](=O)[O-])C1
HCID69042279

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)c1nccc(N2CCCC(O[Si](C)(C)C(C)(C)C)C2)c1N
HCID86669190

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

Following Method 2 of Example 49, (+/−)-4-(3-(tert-butyl dimethylsilyloxy)piperidin-1-yl)-3-nitropyridine in ethanol was reduced yielding tert-butyl (+/−)-4-(3-(tert-butyldimethylsilyloxy)piperidin-1-yl)pyridin-3-amine. LCMS (m/z): 308.2 (MH+); LC Rt=3.47 min.