HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 67119738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,7-Dihydroxynaphthalene-2-carboxylic acid | HCID 19822901 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67119738 | HCID 67119738 | — |
Reaction Steps
K2CO3 (2.88 g, 20.0 mmol), dry DMF (6.4 mL), 1,7-Dihydroxy-naphthalene-2-carboxylic acid (0.635 g, 3.11 mmol), and benzyl chloride (1.72 mL). Yield: 0.805 g of golden brown viscous product (55%, 2 steps).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08822515B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-04b760b2af634a32aba02e9cbaca6552 |
| Source note | uspto-grants-2014_09 |