huagongshe.com
HRID70316

反应详情

EQUATION

反应方程式

HRID 70316 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)c1ccc(B(O)O)cc1
HCID2737811

4-Carbamoylphenylboronic acid

C7H8BNO3

结构：CC(C)(C)OC(=O)N1CCc2ccc(OS(=O)(=O)C(F)(F)F)cc2C1
HCID21250582

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCc2ccc(-c3ccc(C(N)=O)cc3)cc2C1
HCID58276363

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 1,1-dimethylethyl 7-{[(trifluoromethyl)sulfonyl]oxy}-3,4-dihydro-2(1H)-isoquinoline carboxylate (Ex V-17) and 4-(aminocarbonyl)-phenyl boronic acid according to the procedure described for I-VII-9. Tan solid; LC/MS (method A) 2.62 min; m/z 353 (M+H, 75%), 297 ([M-C4H8]+H, 100%).

WORKUP

后处理

  1. customLC/MS (method A) 2.62 min